Vinorelbine-loaded multifunctional magnetic nanoparticles as anticancer drug delivery systems: synthesis, characterization, and in vitro release study

• Zeynep Özcan and
• Afife Binnaz Hazar Yoruç

Beilstein J. Nanotechnol. 2024, 15, 256–269, doi:10.3762/bjnano.15.24

• examining the binding of PEG to PDA/Fe3O4 NPs and the resulting chemical structure using FTIR spectroscopy. According to the FTIR analysis results, the peak at 585 cm–1 in the spectrum corresponds to the vibration associated with the Fe–O bond in magnetic nanoparticles [49]. The peak observed at 3400 cm–1

Assessing phytotoxicity and tolerance levels of ZnO nanoparticles on Raphanus sativus: implications for widespread adoptions

• Pathirannahalage Sahan Samuditha,
• Nadeesh Madusanka Adassooriya and
• Nazeera Salim

Beilstein J. Nanotechnol. 2024, 15, 115–125, doi:10.3762/bjnano.15.11

• on Raphanus sativus (R. sativus) concerning its tolerance levels, toxicity, and accumulation. ZnO NPs were synthesized by the wet chemical method and characterized by powder X-ray diffraction (PXRD), Fourier-transform infrared (FTIR) spectroscopy, ultraviolet–visible (UV–vis) spectroscopy, dynamic

• synthesized ZnO NPs were characterized via several techniques such as powder X-ray diffraction (PXRD), Fourier-transform infrared (FTIR) spectroscopy, solid-UV–vis spectroscopy, dynamic light scattering (DLS), and scanning electron microscopy (SEM). Then the potential phytotoxicity of the synthesized ZnO NPs

Influence of conductive carbon and MnCo₂O₄ on morphological and electrical properties of hydrogels for electrochemical energy conversion

• Sylwia Pawłowska,
• Karolina Cysewska,
• Yasamin Ziai,
• Jakub Karczewski,
• Piotr Jasiński and
• Sebastian Molin

Beilstein J. Nanotechnol. 2024, 15, 57–70, doi:10.3762/bjnano.15.6

• present material functional groups, FTIR spectroscopy in attenuated total reflectance (ATR) mode was used (Bruker Vertex70 FT-IR Spectrometer). The FTIR analysis was carried out in a wavenumber range of 400–4000 cm−1 and with a resolution of 2 cm−1 and eight scans were made for each sample. Transmittance

Isolation of cubic Si₃P₄ in the form of nanocrystals

• Polina K. Nikiforova,
• Sergei S. Bubenov,
• Vadim B. Platonov,
• Andrey S. Kumskov,
• Nikolay N. Kononov,
• Tatyana A. Kuznetsova and
• Sergey G. Dorofeev

Beilstein J. Nanotechnol. 2023, 14, 971–979, doi:10.3762/bjnano.14.80

• FTIR spectroscopy of the etching product are shown in Figure 1). The bands with the wavenumbers of 2105 and 2900 cm−1, and the broad signal at 3400 cm−1 were attributed to vibrations of Si–H, C–H, and O–H bonds, respectively [25]. The IR spectra of the unetched Si NPs display bands in a wavenumber

In situ magnesiothermic reduction synthesis of a Ge@C composite for high-performance lithium-ion batterie anodes

• Ha Tran Huu,
• Ngoc Phi Nguyen,
• Vuong Hoang Ngo,
• Huy Hoang Luc,
• Minh Kha Le,
• Minh Thu Nguyen,
• My Loan Phung Le,
• Hye Rim Kim,
• In Young Kim,
• Sung Jin Kim,
• Van Man Tran and
• Vien Vo

Beilstein J. Nanotechnol. 2023, 14, 751–761, doi:10.3762/bjnano.14.62

• composites were determined using FTIR spectroscopy, as shown in Figure 1b. The FTIR spectra of pure Ge consist of two broad bands in the wavenumber ranges of 500–600 and 800–1000 cm−1. The former band corresponds to the bending modes, and the latter band is attributed to the stretching modes of Ge–O–Ge bonds

Quercetin- and caffeic acid-functionalized chitosan-capped colloidal silver nanoparticles: one-pot synthesis, characterization, and anticancer and antibacterial activities

• Akif Hakan Kurt,
• Elif Berna Olutas,
• Fatma Avcioglu,
• Hamza Karakuş,
• Mehmet Ali Sungur,
• Cansu Kara Oztabag and
• Muhammet Yıldırım

Beilstein J. Nanotechnol. 2023, 14, 362–376, doi:10.3762/bjnano.14.31

• infrared (FTIR) spectroscopy, and transmission electron microscopy (TEM). The characteristic surface plasmon resonance (SPR) absorption band has been found at 417 and 424 nm for Ch/Q- and Ch/CA-Ag NPs, respectively. The formation of a chitosan shell comprising quercetin and caffeic acid, which surround the

• at the higher energy side of the SPR peak of the Ch/CA-Ag NPs while its absorption tail overlaps with that of the SPR peak. These partial matches in the absorption features might be due to the molecular interactions between caffeic acid and chitosan/silver nanostructures [63]. FTIR spectroscopy

Photoelectrochemical water oxidation over TiO₂ nanotubes modified with MoS₂ and g-C₃N₄

• Phuong Hoang Nguyen,
• Thi Minh Cao,
• Tho Truong Nguyen,
• Hien Duy Tong and
• Viet Van Pham

Beilstein J. Nanotechnol. 2022, 13, 1541–1550, doi:10.3762/bjnano.13.127

• determined by using FTIR spectroscopy, as shown in Figure 3b. The formation of TiO2 on the Ti foil is indicated by the vibrations of the Ti–O bond in the wavenumber region from 450 to 750 cm−1 [47]. The bonding characteristics in the MoS2 material are presented by Mo–S vibration peaks between 1620 and 420 cm

• −1 [48]. Also, FTIR spectroscopy is used as an extremely effective technique for studying the vibrational states of organic bonds in g-C3N4 materials using the vibrational peaks of C–N bonds between 1640 and 1200 cm−1. A very strong absorption peak at 807.2 cm−1 characterizes the fluctuation of tri-s

In search of cytotoxic selectivity on cancer cells with biogenically synthesized Ag/AgCl nanoparticles

• Mitzi J. Ramírez-Hernández,
• Mario Valera-Zaragoza,
• Omar Viñas-Bravo,
• Ariana A. Huerta-Heredia,
• Miguel A. Peña-Rico,
• Erick A. Juarez-Arellano,
• David Paniagua-Vega,
• Eduardo Ramírez-Vargas and
• Saúl Sánchez-Valdes

Beilstein J. Nanotechnol. 2022, 13, 1505–1519, doi:10.3762/bjnano.13.124

• /AgCl nanoparticles as observed by FTIR spectroscopy (Figure 5). The reducing species are oxidized and as a consequence have greater thermal stability. Hence, the higher temperature-shifted TGA curves show the thermal behavior of the modified metabolites during chemical reaction. The results are also

Recent advances in green carbon dots (2015–2022): synthesis, metal ion sensing, and biological applications

• Aisha Kanwal,
• Naheed Bibi,
• Sajjad Hyder,
• Arif Muhammad,
• Hao Ren,
• Jiangtao Liu and
• Zhongli Lei

Beilstein J. Nanotechnol. 2022, 13, 1068–1107, doi:10.3762/bjnano.13.93

Electrocatalytic oxygen reduction activity of AgCoCu oxides on reduced graphene oxide in alkaline media

• Iyyappan Madakannu,
• Indrajit Patil,
• Bhalchandra Kakade and
• Kasibhatta Kumara Ramanatha Datta

Beilstein J. Nanotechnol. 2022, 13, 1020–1029, doi:10.3762/bjnano.13.89

• the trimetallic oxide NPs. The graphene oxide support provides the necessary functional groups for the cohesion of binary and ternary metallic oxide NPs (Figure S2a, Supporting Information File 1). The functional groups and the metal oxygen bonds were determined by FTIR spectroscopy, besides the

Antibacterial activity of a berberine nanoformulation

• Hue Thi Nguyen,
• Tuyet Nhung Pham,
• Anh-Tuan Le,
• Nguyen Thanh Thuy,
• Tran Quang Huy and
• Thuy Thi Thu Nguyen

Beilstein J. Nanotechnol. 2022, 13, 641–652, doi:10.3762/bjnano.13.56

• of glycerol on the physicochemical properties of BBR NPs was investigated by UV–vis absorption and FTIR spectroscopy. The UV–vis absorption spectra of pure BBR and BBR NP solutions in distilled water at the same concentration are shown in Figure 1. Glycerol has no absorption band in the UV–vis

• , whereas the solubility of BBR NPs was significantly enhanced. The chemical characteristics of BBR and BBR NPs were analyzed through FTIR spectroscopy (Figure 2). In the FTIR spectrum of glycerol (Figure 2a), the absorption band appearing at 3287 cm−1 is characteristic for stretching vibrations of the –OH

Boosting of photocatalytic hydrogen evolution via chlorine doping of polymeric carbon nitride

• Malgorzata Aleksandrzak,
• Michalina Kijaczko,
• Wojciech Kukulka,
• Daria Baranowska,
• Martyna Baca,
• Beata Zielinska and
• Ewa Mijowska

Beilstein J. Nanotechnol. 2021, 12, 473–484, doi:10.3762/bjnano.12.38

• the interlayers of PCN and not on its π-conjugated planes as it is in the case with other commonly used metal/non-metal (Cu, Ni, C, N or O) modifications [42][43][44][45][46]. Fourier-transform infrared (FTIR) spectroscopy was used to obtain the molecular structure information of the carbon nitride

A review on the green and sustainable synthesis of silver nanoparticles and one-dimensional silver nanostructures

• Sina Kaabipour and
• Shohreh Hemmati

Beilstein J. Nanotechnol. 2021, 12, 102–136, doi:10.3762/bjnano.12.9

• spherical in morphology and range from 5–200 nm in size. The mechanism through which AgNPs are synthesized is still not well understood; however, Fourier-transform infrared (FTIR) spectroscopy results from previous studies suggest that carboxylic and hydroxylic groups, in addition to primary and secondary

Transient coating of γ-Fe₂O₃ nanoparticles with glutamate for its delivery to and removal from brain nerve terminals

• Konstantin Paliienko,
• Artem Pastukhov,
• Michal Babič,
• Daniel Horák,
• Olga Vasylchenko and
• Tatiana Borisova

Beilstein J. Nanotechnol. 2020, 11, 1381–1393, doi:10.3762/bjnano.11.122

• the ligands. Raman and FTIR spectroscopy measurements showed that glutamate and aspartate salts were adsorbed at the surface of γ-Fe2O3 nanoparticles [20]. It should be noted that the methodological protocol of above experiments on glutamate and aspartate chemisorption suggested the use of bio

Silver-decorated gel-shell nanobeads: physicochemical characterization and evaluation of antibacterial properties

• Marta Bartel,
• Katarzyna Markowska,
• Marcin Strawski,
• Krystyna Wolska and
• Maciej Mazur

Beilstein J. Nanotechnol. 2020, 11, 620–630, doi:10.3762/bjnano.11.49

• the particles is similar to that of non-sulfonated polystyrene beads (SEM data not shown). Thus, if shape and size of the beads are retained during the reaction, the question arises whether they have been in fact transformed into the gel-shell particles [27][28]. To answer this question FTIR

• spectroscopy has been employed. Figure 3 shows the FTIR spectrum of the sulfonated particles. The most intense mode at 1186 cm−1 with a broad shoulder is attributed to the asymmetric stretching of S=O bonds. The symmetric stretching vibrations of SO3− groups produce the band at 1041 cm−1. The peak at 834 cm−1

Electrochemically derived functionalized graphene for bulk production of hydrogen peroxide

• Munaiah Yeddala,
• Pallavi Thakur,
• Anugraha A and
• Tharangattu N. Narayanan

Beilstein J. Nanotechnol. 2020, 11, 432–442, doi:10.3762/bjnano.11.34

• (see Figure 2a). In order to test the durability of the materials in acidic medium, chronoamperometry studies were carried out in 0.5 M H2SO4 at 0.45 V vs RHE for 3 h. The EEG samples were studied (before and after chronoamperometry) using Raman and FTIR spectroscopy along with the electrochemical

• lab 2000) and FTIR spectroscopy were used to unravel the nature and degree of functionalization along with the change in morphology of these samples. The surface area of the samples was analyzed using Brunauer–Emmett–Teller (BET) adsorption isotherms from a Quantachrome Nova 1200e surface area

Synthesis and enhanced photocatalytic performance of 0D/2D CuO/tourmaline composite photocatalysts

• Changqiang Yu,
• Min Wen,
• Zhen Tong,
• Shuhua Li,
• Yanhong Yin,
• Xianbin Liu,
• Yesheng Li,
• Tongxiang Liang,
• Ziping Wu and
• Dionysios D. Dionysiou

Beilstein J. Nanotechnol. 2020, 11, 407–416, doi:10.3762/bjnano.11.31

• to pure CuO, the binding energy of Cu 2p3/2 and Cu 2p1/2 for the CuO/tourmaline composite was shifted to 933.49 eV and 953.37 eV, respectively, providing evidence of the chemical interaction between CuO and tourmaline. It is convenient to detect the chemical bonds in complex materials by FTIR

• spectroscopy. As shown in Figure 2, three bands appeared at 3487 cm−1, 3554 cm−1, and 3635 cm−1 resulting from the vibration of the three OH groups in tourmaline [2]. The bending vibration of the Si–O group was detected at 488 cm−1 [27]. The band at 649 cm−1 was due to the RIV–O (R = Al, Fe, Mg, Mn) stretching

Size effects of graphene nanoplatelets on the properties of high-density polyethylene nanocomposites: morphological, thermal, electrical, and mechanical characterization

• Tuba Evgin,
• Alpaslan Turgut,
• Georges Hamaoui,
• Zdenko Spitalsky,
• Nicolas Horny,
• Matej Micusik,
• Mihai Chirtoc,
• Mehmet Sarikanat and
• Maria Omastova

Beilstein J. Nanotechnol. 2020, 11, 167–179, doi:10.3762/bjnano.11.14

• chemical composition of GnPs, as determined by XPS. DSC results for the HDPE/GnP nanocomposites. Results of the TGA analysis of the HDPE/GnP nanocomposites. Sizes of GnPs used in this study. Supporting Information Supporting Information File 90: FTIR spectroscopy and XRD patterns of HDPE/GnP

Fully amino acid-based hydrogel as potential scaffold for cell culturing and drug delivery

• Dávid Juriga,
• Evelin Sipos,
• Orsolya Hegedűs,
• Gábor Varga,
• Miklós Zrínyi,
• Krisztina S. Nagy and
• Angéla Jedlovszky-Hajdú

Beilstein J. Nanotechnol. 2019, 10, 2579–2593, doi:10.3762/bjnano.10.249

• shrink. Between pH 6 and 8, the swelling degrees abruptly rise as the polymer networks are hydrolyzed. The successful hydrolysis was proved by FTIR spectroscopy (Supporting Information File 1, Figure S2). This kind of abrupt change was described in previous articles, where other molecules or only LYS

Multiwalled carbon nanotube based aromatic volatile organic compound sensor: sensitivity enhancement through 1-hexadecanethiol functionalisation

• Nadra Bohli,
• Meryem Belkilani,
• Juan Casanova-Chafer,
• Eduard Llobet and
• Adnane Abdelghani

Beilstein J. Nanotechnol. 2019, 10, 2364–2373, doi:10.3762/bjnano.10.227

• performance [25][26]. FTIR characterisation In order to ensure that the HDT monolayers are formed and well immobilized on the Au-MWCNT layers, we used FTIR spectroscopy. Figure 3 shows the infrared spectra, in absorbance mode, of both Au-MWCNT and HDT/Au-MWCNT layers. When analysing and comparing the infrared

Improved adsorption and degradation performance by S-doping of (001)-TiO₂

• Xiao-Yu Sun,
• Xian Zhang,
• Xiao Sun,
• Ni-Xian Qian,
• Min Wang and
• Yong-Qing Ma

Beilstein J. Nanotechnol. 2019, 10, 2116–2127, doi:10.3762/bjnano.10.206

• probed by Fourier-transform infrared (FTIR) spectroscopy (Vertex 80/Hyperion2000, Bruker, Germany). The Brunauer–Emmett–Teller (BET) specific surface areas were calculated based on the N2 adsorption–desorption isotherms measured at 77 K using a gas adsorption apparatus (Autosorb-iQ, Quantachrome

Porous silver-coated pNIPAM-co-AAc hydrogel nanocapsules

• William W. Bryan,
• Riddhiman Medhi,
• Maria D. Marquez,
• Supparesk Rittikulsittichai,
• Michael Tran and
• T. Randall Lee

Beilstein J. Nanotechnol. 2019, 10, 1973–1982, doi:10.3762/bjnano.10.194

• of pDADMAC on the hydrogel particle surface, we analyzed the particles with Fourier transform infrared (FTIR) spectroscopy. Figure 1f shows the absorption spectra of pure pDADMAC and the modified hydrogel particles. The existence of stretching associated with the CH3 components at ≈1465 cm−1 and

Long-term entrapment and temperature-controlled-release of SF₆ gas in metal–organic frameworks (MOFs)

• Hana Bunzen,
• Andreas Kalytta-Mewes,
• Leo van Wüllen and
• Dirk Volkmer

Beilstein J. Nanotechnol. 2019, 10, 1851–1859, doi:10.3762/bjnano.10.180

• of a guest released from a porous material. The determined value of the activation energy was further compared to the results obtained from computational simulations (see the dedicated section later in the text). To qualify the guest, we used FTIR spectroscopy (Figure 2 and Figure S5 in Supporting

• (to quantify the amount of the guest in MFU-4, Figure 6), powder XRD measurements (Figure S6 in Supporting Information File 1) and FTIR spectroscopy (Figure 7 and Figure S7 in Supporting Information File 1). Based on the results of these measurements, it can be concluded that there was no leaking of

• the guest. Both TGA (Figure 6 and Table 2) and FTIR spectroscopy (Figure 7, and Figure S8 and Table S1 in Supporting Information File 1) showed that SF6 remained inside the pores over the entire investigated period. The analyses also revealed that upon exposure of the sample to air, a small amount of

Layered double hydroxide/sepiolite hybrid nanoarchitectures for the controlled release of herbicides

• Ediana Paula Rebitski,
• Margarita Darder and
• Pilar Aranda

Beilstein J. Nanotechnol. 2019, 10, 1679–1690, doi:10.3762/bjnano.10.163

• at mild temperatures below 150 °C. FTIR spectroscopy also confirms the incorporation of MCPA through interaction with the LDH (Figure S3, Supporting Information File 1), as discussed for the hybrid nanoarchitectures prepared by ion exchange. The FE-SEM images of the MCPA-LDH/Sep hybrid

Chiral nanostructures self-assembled from nitrocinnamic amide amphiphiles: substituent and solvent effects

• Hejin Jiang,
• Huahua Fan,
• Yuqian Jiang,
• Li Zhang and
• Minghua Liu

Beilstein J. Nanotechnol. 2019, 10, 1608–1617, doi:10.3762/bjnano.10.156

• self-assembled molecules, FTIR spectroscopy was employed to evaluate the formation mechanism of self-assembly. As shown in Figure 5, for the 2NCLG and 4NCLG assemblies, two absorption bands at ≈3330 cm−1 and ≈3284 cm−1 were observed, which can be ascribed to the N–H stretching vibration. While for

• formed in ethanol (Supporting Information File 1, Figure S3). These results indicated that the choice of solvent had a significant effect on the formed nanostructures. To support our speculation, the 3NCLG assemblies in DMF and THF were monitored by FTIR spectroscopy, as shown in Figure 8. We mainly

• /Max-2500 X-ray diffractometer (Japan) with Cu Kα radiation (λ =1.5406 Å). The operating voltage was 40 kV and a current of 200 mA was used. The samples were cast on silicon substrates and dried in air for XRD measurements. Fourier-transform infrared (FTIR) spectroscopy was recorded with a Bruker